Der neutrale lipophile Titelkomplex (I) wird durch Reduktion von Ammoniumpertechnetat (99Tc) mit K‐tetrahydridoborat in wäßriger 3 M HCl‐Lösung in Gegenwart von K‐hydrido‐tris‐[ l‐pyrazolyl]‐borat dargestellt und durch IR‐, Raman‐ sowie NMR‐Spektren charakterisiert.
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