There has been interest in the use of plant extract as a natural preservative agent for improving the oxidative stability of vegetable oils. However, plant extracts have low stability against heat and environmental stress. In this study, the antioxidant potential of nano‐ and microencapsulated Rosmarinus officinalis L. extract (RE) obtained using the ultrasonication method was measured. The total phenolic and flavonoid content of the extract was 174.4 ± 25.9 mg gallic acid/g extract and 78.30 ± 3.2 mg rutin/g extract, respectively. Antioxidant activity of 50, 100, 200, and 400 ppm of RE was measured by DPPH free radical scavenging methods, ferric reduction assay, and β‐carotene/linoleic acid assay, and then compared to the 100 ppm of TBHQ as a common synthetic antioxidant. The results showed that the antioxidant activity increased with increasing the concentration of the extract in all evaluating methods. The antioxidant activity of 200 ppm of the free and encapsulated extract in cress (Lepidium sativum) and basil (Ocimum basilicum) seed gums at different ratios (1:0, 1:1, and 0:1) was compared to sunflower oil without antioxidants, and oil‐containing TBHQ which was stored at 60°C for 24 days. The oxidation indexes of oil samples include peroxide value, thiobarbituric acid value, and p‐anisidine value measured at 4‐day intervals. A lower oil oxidation was observed in oil‐containing nanoencapsulated extract followed by microencapsulated extract, free extract, and TBHQ. Since producing nanoencapsulated RE requires a higher time and speed of homogenization and due to no statistically significant difference between the antioxidant properties of nanocapsules and microcapsules in oil, the use of microcapsules of RE in basil seed gum to increase the shelf life of sunflower oil is recommended.
Various garlic nutrients bring about several health benefits. Allicin, the major bioactive component of garlic, has anticancer, antimicrobial, antioxidant, cardiovascular-preventive, and cholesterol-reducing effects. Using water as the solvent, the ultrasound-assisted extraction of garlic compounds were optimized through response surface methodology (RSM). The process was conducted at different times (10-30 min), temperatures (30-60°C), frequencies (37 and 80 Hz), and powers (40-100 W). The obtained extracts were assessed for DPPH scavenging activity, total phenolic content (TPC), and extraction efficiency. The optimal conditions were 10 min, 30°C, 37 Hz, and 40 W (R 2 = 0.93 for the DPPH assay, R 2 = 0.99 for the TPC, and R 2 = 0.94 for the extraction efficiency). Sonication time and temperature most affected the responses. In conclusion, ultrasound could be easily utilized for the extraction, because it accelerated the process and lowered the extraction time, which enhanced the extract quality with regards to antioxidant properties and the likelihood of extracting heat-sensitive substances.
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.