The enhancement of the fatigue strength is significant for the engineering applications of commercial pure titanium and its alloys. The paper investigated improvement of fatigue strength for commercial pure titanium by combined high-energy shot peening. Firstly, nano-crystallization in surface layer of pure titanium was carried out by high-energy shot peening, and then the shot peening with small diameter shots was introduced to degrade the surface roughness, enhancing the quality of the nano-grained surface. The fatigue limit of pure titanium by high-energy shot peening turns out to be increased by 34%, and the fatigue limit of pure titanium by compound high-energy shot peening turns out to be increased by 52.3%, according to the results. Effective factors such as surface states etc. to fatigue life, the fatigue crack initiation and propagation behaviors were also discussed in this paper.
The main factor of rubber fatigue was stress field. But the way is not sensitive in many cases. To clarify which factors were the main for predict the locations of fatigue crack, we analyzed the factors of stress field and strain field of rubber joint, and relations between the factors and the locations of fatigue crack, using 3D FE simulation. The result showed stress concentration was not sensitive to predict the locations of fatigue crack. The locations are close to strain concentration of rubber joint. In this paper we propose the approach of using strain concentration to predict the fatigue crack locations for rubber joint. This result is significant for the rubber joint design and the study of fatigue strength theoretic.
The paper investigated nano-crystallization on surface layer of commercial pure titanium by using high-energy shot peening. The grain size and the microstructure in deformed surface layer by high-energy shot peening are analyzed with X-ray diffraction and TEM etc. In addition, the variations of surface microhardness are examined after high-energy shot peening. The results described that the nano-crystalline surface layer have been formed in commercial pure titanium with a structure of hexagonal closet packet, by high-energy shot peening. The surface microhardness increases and the grain size in nano-crystalline surface layer diminishes, with increasing the time in high-energy shot peening. The minimum nano-crystalline grain size is approximately 40 nm.
The rotary bending fatigue tests were to investigate the effect of the combined shot peening for surface nanocrystallization (CSPN) on the fatigue limit of titanium (TC4). CSPN formed nano-crystallization in surface layer of TC4, and may reduce and reducing the surface damage of TC4 by high energy shot peening. In the case of equiaxed microstructure, the fatigue limit of TC4 specimen treated by high-energy shot peening is increased by 13%, while the fatigue limit of TC4 specimen treated by the CSPN is increased by 34%. But in the case of lamellar microstructure, the fatigue limits of the specimens by either the surface treatment process both of the high energy shot peening and CSPN. The main reason of fatigue improvement change is due to that the effect of surface nanocrystallization and surface damage repairing by CSPN is changed between the different microstructure of TC4.
Yb3+ and Ho3+ co-doped Lu2O3 nanocrystalline powders were synthesized by a reversestrike co-precipitation method. The as-prepared powders were examined by the X-ray diffraction and transmission electron microscopy. The phase composition of the powders was cubic and the particle size was in the range of 30~50 nm. Emission and excitation spectra of the powders were measured by a spectrofluorometer and the possible upconversion luminescence mechanism was also discussed.
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