A facile synthesis method was developed based on the seed-mediated growth to get the narrow dispersed silver nanoparticles with controllable sizes ranging from 20 nm to larger than 120 nm. Environmentally friendly glucose acts as a reducing agent. Because of its weak reducing ability, the secondary nucleation is prevented in the seed-mediated growth, and the size of silver nanoparticles can be tuned continuously by the continuous addition of reactants. Controlling the supersaturation level is critical to suppress both the nucleation and Ostwald ripening, which can be realized by carefully controlling the addition rate of the reactants. We also set up a convenient method to determine the size and size-distribution of silver nanoparticles from the size-dependent absorption spectra of the colloids, and optimize the growth parameters using this method to get narrow dispersed silver nanoparticles.
Transparent copper nanorod/nanowire arrays and anodic alumina oxide composite films have been prepared by alternating current electrodeposition, and their linear optical properties have been systematically characterized by absorption spectra. In the experimental spectra, there exist transverse and longitudinal resonance peaks, which are caused by the surface-plasmon resonance along the diameter and the length of the copper nanorods, respectively. The transverse resonance peak is affected by the diameter and aspect ratio of the nanorod. The longitudinal resonance peak appears at longer wavelength when a polarized light illuminates the film with an angle of incidence of about 70 degrees , where the angle is defined with respect to the surface normal. Moreover, the longitudinal resonance mode is sensitive to the polarization direction when compared with the transverse resonance mode.
HCDs–DOX was prepared with low cytotoxicity, and sustained, pH-targeted release properties. In vitro release conformed to the Weibull model and Fick diffusion.
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