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This contribution characterizes the performance of a DESI 11 high-speed disintegrator working on the principle of a pin mill with two opposite counter-rotating rotors. As the ground material, batches of Portland cement featuring 6–7 Mohs scale hardness and containing relatively hard and abrasive compounds with the specific surface areas ranging from 200 to 500 m2/kg, with the step of 50 m2/kg, were used. The character of the ground particles was assessed via scanning electron microscopy and measurement of the absolute/relative increase in their specific surface areas. Detailed characterization of the rotors was performed via recording the thermal imprints, evaluating their wear by 3D optical microscopy, and measuring rotor weight loss after the grinding of constant amounts of cement. The results showed that coarse particles are ground by impacting the front faces of the pins, while finer particles are primarily milled via mutual collisions. Therefore, the coarse particles cause higher abrasion and wear on the rotor pins; after the milling of 20 kg of the 200 m2/kg cement sample, the wear of the rotor reached up to 5% of its original mass and the pins were severely damaged.

The paper deals with the mechanical activation of cement by grinding in a high-speed mill, and compares the parameters found with the commonly used grinding method in cement production, which uses grinding of cement by means of a ball mill. The aim is to verify the influence of the aging time of the ground material on the preservation of the mechanical activation effect and on the properties of the final product at different stages of hydration. It evaluates the physical-mechanical properties, the compressive and tensile strength after 1, 2, 7, 14 and 28 days, as well as the course of the hydration process. The evaluated results suggest the existence of mechanical activation, but this effect is very difficult to achieve and depends on many other factors.

This article deals with the preparation and laboratory milling of β-dicalcium silicate. Dicalcium silicate is the second most important calcium silicate of Portland clinker. β-C2S is usually dominated in industrially produced clinker. Pure β-C2S can be prepared in several ways. Traditional way is the solid phase synthesis of raw material mixture. The paper deals with the preparation of β-dicalcium silicate, which is based on the modified Wesselsky-Jensen method and with the influence of length and the technology of the milling process in 3 types of laboratory mills on the particle size, distribution and agglomeration of the synthetically prepared β-dicalcium silicate.