Titania gel was synthesized by sol-gel method and dehydration kinetics of the gel was studied using a thermo gravimetric analyzer in the temperature range of 35-700 o C at three different heating rates. Dehydration of the gel was observed to take place at two different stages. Kinetic analysis for dehydration at both stages were performed by Friedman model fitting and Kissinger -Akahira -Sunose (KAS) model free methods to determine kinetic triplet. It was observed that dehydration of the titania gel sample followed second order reaction kinetics in both the stages.