Background: Through this research work prepared two different variety of Homoeopathic medicated hair oil by mixing Robinia, Embelica officinalis and Jaborandi mother tincture in a coconut oil as simplex and complex variety which undergoes into qualitative analysis done by UV-VIS spectrophotometer. Methodology: For the preparation of Homoeopathic medicated Hair oil as simplex and complex variety. The drug and vehicle ratio should be taken as (1:9) with virgin coconut oil as 9 part and Jaborandi, robinia, Emeblica officinalis mother tincture as 1 part, which undergoes into the indirect heating under Hot water bath at 80 °C Until and unless the solution became homogeneous. Afterwards filter with Filter paper and taken as 1 part of it and again mixed with 9 parts of virgin olive oil as a vehicle. Prepared the simplex variety by mixing Jaborandi-Q, Embelica-Q and Robinia-Q in virgin coconut oil separately, whereas prepared mixed variety of Homoeopathic Medicated hair oil by mixing Jaborandi-Q, Embelica officinalis-Q and Robinia-Q in virgin coconut oil in a equal proportion and Filled into the hard glass bottles for observation under 15 days. Results: These samples were passes under the UV-visible spectrophotometer (Double beam) through which absorbance value of Jaborandi hair oil is 0.191 at 413.00 nm, 0.062 at 499.00 nm, Absorbance value of Emeblica officinalis Q is 0.048 at 698.00 nm, Robinia Hair oil is 0.092 at 699.00 nm, Mixed variety of Homoeopathic hair oil is 0.066 at 699.00 nm, Jaborandi Q is 0.662 at 608.00 nm and Embelica officinalis is 0.977 at 562.00 nm and Robinia Q is 0.985 at 552.00 nm.