International audienceAs expected from the alloy design procedure, combined Twinning Induced Plasticity (TWIP) and Transformation Induced Plasticity (TRIP) effects are activated in a metastable β Ti-12(wt.%)Mo alloy. In-situ Synchrotron X-ray diffraction (XRD), electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM) observations were carried out to investigate the deformation mechanisms and microstructure evolution sequence. In the early deformation stage, primary strain/stress induced phase transformations (β->ω and β->α'') and primary mechanical twinning ({332}<113> and {112}<111>) are simultaneously activated. Secondary martensitic phase transformation and secondary mechanical twinning are then triggered in the twinned β zones. The {332}<113> twinning and the subsequence secondary mechanisms dominate the early stage deformation process. The evolution of the deformation microstructure results in a high strain hardening rate (~2GPa) bringing about high tensile strength (~1GPa) and large uniform elongation (> 0.38)

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