In this paper, nearly monodispersed urchinlike Ni powders were synthesized by a simple hydrogen-thermal reduction method. Electromagnetic and absorption characteristics were then investigated at 0.5–18 GHz. The permeability spectra present four resonance peaks over the whole frequency range. The resonance absorption property was discussed by fitting the permeability spectrum using the well-known Landau-Lifshitz-Gilbert equation and Maxwell-Garnett mixing rule. Correspondingly, the magnetic loss of the first band observed is attributed to the natural resonance, while the other three bands are considered to originate from non-uniform exchange resonance in the permeability spectra. The maximum reflection loss can reach −43 dB at about 10 GHz with 2 mm in absorber thickness.

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