Polycrystalline rubidium superoxide (RbO2) has been synthesized by using solution method followed by the reaction process under the cooling condition of-40 °C. X-ray Powder Diffraction (XRD) spectra showed that RbO2 was successfully synthesized by this method. The magnetic susceptibility and pulsed muon spin relaxation (μSR) measurements were carried out in order to study the magnetic properties of RbO2.
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