ObjectiveTo evaluate the influence of solvent evaporation in the kinetics of water
diffusion (water sorption-WS, solubility-SL, and net water uptake) and nanoleakage
of adhesive systems. Material and MethodsDisk-shaped specimens (5.0 mm in diameter x 0.8 mm in thickness) were produced
(N=48) using the adhesives: Clearfil S3 Bond (CS3)/Kuraray, Clearfil SE
Bond - control group (CSE)/Kuraray, Optibond Solo Plus (OS)/Kerr and Scotchbond
Universal Adhesive (SBU)/3M ESPE. The solvents were either evaporated for 30 s or
not evaporated (N=24/per group), and then photoactivated for 80 s
(550 mW/cm2). After desiccation, the specimens were weighed and stored
in distilled water (N=12) or mineral oil (N=12) to evaluate the water diffusion
over a 7-day period. Net water uptake (%) was also calculated as the sum of WS and
SL. Data were submitted to 3-way ANOVA/Tukey's test (α=5%). The nanoleakage
expression in three additional specimens per group was also
evaluated after ammoniacal silver impregnation after 7 days of water storage under
SEM. ResultsStatistical analysis revealed that only the factor "adhesive" was significant
(p<0.05). Solvent evaporation had no influence in the WS and SL of the
adhesives. CSE (control) presented significantly lower net uptake (5.4%). The
nanoleakage was enhanced by the presence of solvent in the adhesives. ConclusionsAlthough the evaporation has no effect in the kinetics of water diffusion, the
nanoleakage expression of the adhesives tested increases when the solvents are not
evaporated.
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