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In this work, g-C 3 N 4 /TiO 2 nanocatalysts were prepared by high-voltage electrospinning and hydrothermal methods. The surface of the pure TiO 2 nanomaterial was treated by acidification before it was combined with g-C 3 N 4 .Various characterization methods were used to characterize the prepared photocatalyst. RhB (20 mg/L) was degraded as a target-degradable pollutant, the degradation efficiency of the nanocatalyst was measured under UV-Visible light. The results show that the degradation efficiency of the g-C 3 N 4 / TiO 2 nanocomposite material that has undergone pre-acidification treatment is much higher than that of the untreated catalyst.

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