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The form‐stabilized phase change materials (PCMs) comprised of lauric acid (LA), high‐density polyethylene (HDPE) and graphene nanoplates‐carbon nanofibers (GNP‐CNF) hybrid fillers were synthesized by melt blending method in this work, and the effects of GNP‐CNF mass ratio on thermal properties were investigated. The results from FT‐IR and XRD reveal that LA, HDPE, GNP and CNF were integrated with each other in a physical manner. The LA/HDPE/GNP‐CNF composites possess melting points very close to that of pure LA, with melting latent heats of 113.83–119.84 J/g. Thermal conductivity results indicate that the effect of GNP is better than that of CNF at the same content. The synergistic effect of hybrid carbon fillers can achieve higher thermal conductivity value compared to a single GNP or CNF. The synergistic thermal conductivity improvement mechanism is also analyzed. The sample SN2 (GNP: CNF is 1.7:0.3) exhibits the best thermal conductivity of 0.759 W/(m·K), with 2.73 times that of SN0. It also presents satisfactory thermal stability and reliability, allowing it to have promising applications in thermal energy storage.

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