A synchrotron technique, differential aperture X-ray microscopy (DAXM), has been applied to characterize the microstructure and analyze the local mesoscale residual elastic strain fields around graphite nodules embedded in ferrite matrix grains in ductile cast iron. Compressive residual elastic strains are measured with a maximum strain of ~ 6.5-8 × 10-4 near the graphite nodules extending into the matrix about 20 µm, where the elastic strain is near zero. The experimental data are compared with a strain gradient calculated by a finite element model, and good accord has been found but with a significant over prediction of the maximum strain. This is discussed in terms of stress relaxation during cooling or during storage by plastic deformation of the nodule, the matrix or both. Relaxation by plastic deformation of the ferrite is demonstrated by the formation of low energy dislocation cell structure also quantified by the DAXM technique.
In this paper, the thermo-elastic behavior of the graphite nodules contained in ductile iron is derived on the basis of recent transmission electron microscopy investigations of their real internal structure. The proposed model is initially validated by performing a finite element homogenization analysis to verify its consistency with the room-temperature elastic properties of ductile iron measured at the macro scale. Subsequently, it is used to investigate the formation of local residual stresses around the graphite particles by simulating the manufacturing process of a typical ferritic ductile iron grade, and the results are compared with preliminary measurements using synchrotron X-rays. Finally, the obtained accurate description of the stress & strain field at the micro scale is used to shed light on common failure modes reported for the nodules and on some peculiar properties observed in ductile iron at both micro and macro scale.
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