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Two methoxycarbonyl-substituted 2,5-di(1,3-dithiol-2-ylidene)-1,3-dithiolane-4-thione derivatives with alkylsulfanyl groups of different sizes were synthesized, and their redox and electronic properties and crystal structures were investigated. The difference in the solid-state absorption spectra occurs because of differences in the intermolecular interactions caused by their molecular packings.

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Facile Synthesis of α-Amino Phosphonates in Water by Kabachnik-Fields Reaction Using Magnesium Dodecyl Sulfate. -The three-component synthesis of the title compounds (IV), (VII), and (XI) by using an easily available catalyst is presented. The reaction of aliphatic aldehydes or aliphatic amines with compound (X) proceeds more effectively in the presence of magnesium dodecyl sulfate and Et3N. -(ANDO*, K.; EGAMI, T.; Heteroat. Chem. 22 (2011) 3-4, 358-362, http://dx.