In this study, Hardox 400 steel used as substrate material was coated through solid media Thermoreactive Diffusion (TRD) method using Ferro Niobium and Ferro Boron powders from carbide forming element powders. Coating was carried out in three different temperatures ([Formula: see text]C, [Formula: see text]C and [Formula: see text]C) and three different time intervals (1, 2 and 3[Formula: see text]h). Microstructures of the coated specimens were examined by optical microscope, Scanning Electron Microscope (SEM), Energy Dispersive X-Ray Spectroscopy (EDX) and X-ray Diffraction (XRD); and hardness values were measured. The effects of coating parameters on coating thickness and hardness were analyzed by ANOVA. In addition, specimens were subjected to wear tests to determine the effect of hardness and coating parameters on wear. In the wear tests, Taguchi test design setup was used. The obtained results were compared with the Hardox 400 steel used under current conditions. It was seen from optical microscope and SEM images that Hardox 400 steel surface could be coated with TRD method depending on coating parameters. The average thickness of NbC–B coating ranged from 1.797[Formula: see text][Formula: see text]m to 5.596[Formula: see text][Formula: see text]m under different process temperature and time. Rising the coating time and temperature increased the coating thickness by 311.40%. EDX analysis showed that the coating layer was composed of B, C, Fe and Nb elements, and XRD analysis also showed that the phase in the coating layer is NbC–B. The NbC–B phase was determined to be an important factor in increasing the hardness. The coating hardness is enhanced by 320.80% depending on the coating parameters. Optimum coating thickness, hardness and wear results were obtained from high coating temperature and time. Uncoated Hardox 400 steels were worn out more compared to the coated Hardox 400 steels. The contribution of coating temperature and time to wear resistance was 1.46% and 8.02%, respectively. It was observed that the important parameter for wear volume was the applied load.
In this study, FeCrC powder was alloyed on the surface of AISI 1030 steel with FeCrC powder having 70% Cr ratio with the Plasma Transferred Arc Welding Method. In the coating process performed with the Plasma Transferred Arc Welding Method, N 2 gas at 1-3-5% ratio was added to the shielding gas. The coating layer was analysed using optical microscope (OM), scanning electron microscope (SEM), X-ray diffractogram (XRD) and X-ray energy dispersive spectrometer (EDS). As a result of optical microscope and microstructure analyses, it was determined that the coating layer and the sub-layer were connected to each other metallurgical and there were austenite (γ), Fe-Cr, Fe 23 (C) 6 , and Cr 7 C 3 phase and carbides and CrN in the structure.Keywords: Plasma transferred arc coating; surface modifications; chromium carbide; chromium nitrurs; microstructure W pracy badano nakładanie powłok z proszku FeCrC o zawartości 70% chromu na powierzchni stali AISI 1030 metodą PTA. W czasie nakładania powłoki zawartość azotu w gazie ochronnym wynosiła 1, 3, 5%. Uzyskane powłoki badane były za pomocą mikroskopii optycznej, skaningowej mikroskopii elektronowej, dyfrakcji rentgenowskiej i mikroanalizy rentgenowskiej. W oparciu o wyniki obserwacji i analiz mikrostruktury stwierdzono, że powłoka i warstwa pośrednia połączone są ze sobą metalurgicznie. Stwierdzono obecność austenitu, Fe-Cr, Fe 23 (C) 6 , Cr 7 C 3 oraz węglików i CrN w mikrostrukturze.
In this study, B4C and FeCrC powders were alloyed on the surface of AISI 430 by a fusion process via plasma transferred arc welding. Mixtures of these powders at various amounts were used. The microstructure and wear behavior of the obtained coating layers were investigated. The wear behavior of the coating layers was planned using the Taguchi method. Abrasive wear mass loss results were optimized with the “smaller the better” control characteristic of the Taguchi method, and the results were analyzed graphically. The actual data obtained at the end of the study were formed by using an L16 (4 × 2, 2 × 2) mixed array, and the remaining wear rates were calculated with the help of theoretical formulas in order to obtain theoretical abrasive wear results.
The purpose of this study is to investigate the effects of process parameters on adhesive wear resistance by using the Taguchi experimental design method. In this study, Cu-Ni/B4Cp composites were produced by the powder metallurgy method and the effect on the adhesive wear resistance was investigated. Cu-Ni/B4Cp composite materials were made by cold pressing methods and reinforced with 1% Ni as well as with 6, 12 and 18% B4Cp, respectively. The sintering was carried out at 800 and 900°C for 60 minutes. The wear tests were performed by using block on ring test apparatus at loads of 5, 10 and 15 N at a rotation speed of 90 rpm and a wear distance of 250, 500 and 750 m, respectively. The results were evaluated by the calculated wear losses. The wear resistance increased with increasing B4C ratio.
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