The article presents the results of the investigation of the process of concentrating solutions of low-volatile liquids in a flowing film under the conditions of evaporation in the cross-flow of neutral gas. The purpose of the study was to establish the features of solution composition change along the film length. The study was carried out using the developed mathematical model with experimental determination of model parameters: heat and mass transfer coefficients. It was found that at the beginning of the film, the change in the concentration of the solution has a character close to linear, and then the concentration sharply increases until the solvent evaporates completely. It was shown that this pattern of change in the composition of the solution is related to the distribution of the temperature of the solution along the length of the film. The intensity of the concentration process increases with decreasing initial flow rate of the solution and its initial concentration as well as with increasing initial temperature of the solution, initial temperature of the gas and temperature of the surface of the wall along which the film flows. The concentration intensity decreases with an increase in the velocity of the gas entering the space above the film. Comparison of the calculation results concerning aqueous glycerol solution with the experimental data showed their good agreement. The data obtained in the article allow calculating the height of the film concentrator nozzle at which a given concentration of the solution is provided.