Cobalt ferrite is a ferrimagnetic magnetostrictive ceramic that has potential application in magnetoelastic and magnetoelectric transducers. In this work, CoFe2O4 was obtained using a conventional ceramic method and Bi2O3 was used as additive in order to obtain liquid-phase sintered samples. Bi2O3 was added to the ferrite in amounts ranging from 0.25 mol% to 0.45 mol% and samples were sintered at 900 °C and 950 °C. It was observed the presence of Bi-containing particles in the microstructure of the sintered samples and the magnetostriction results indicated microstructural anisotropy. It was verified that it is possible to get dense cobalt ferrites, liquid-phase sintered, with relative densities higher than 90% and with magnetostriction values very close to samples sintered without additives.
Abstract-Pulsed-current sensors require transducers constituted of magnetic materials with high magnetic permeability in a frequency range compatible with the period and the frequency of the current pulse. The use of ferrites in this application has the advantage of low cost and low losses in high frequencies. The aim of this work is to present a procedure for selection of the ceramic processing route of Ni-Zn ferrite for application in a pulsed-current sensor. The ferrite samples were prepared under different processing parameters and characterized in terms of microstructure, chemical analysis, complex magnetic permeability, and magnetic hysteresis. The chosen processing route included high energy milling of the pre-sintered powder, its disaggregation before sample forming, and sintering of the samples in air for 2 h at 1300 • C. Tests were performed and it was verified that using this processing route for the fabrication of the sensor's core it was possible to monitor pulses of 0.1-1.0 µs.
Abstract-This work investigates the variation of the real part of the complex magnetic permeability of a Ni-Zn ferrite for application to temperature sensors. Ferrite samples were fabricated by means of the conventional ceramic method. Zinc, nickel and iron oxides were used as raw materials. The samples were sintered at 1200, 1300, and 1400 • C. The complex magnetic permeability of the samples was measured at temperatures ranging from −40 • C to +50 • C. The complex magnetic permeability of the samples was analyzed in the 100 kHz-100 MHz frequency range, and the temperature sensitivity of the magnetic permeability (∂µ r /∂T ) was analyzed at 100 kHz. The magnetic permeability variation of the ferrite permits to use it as a temperature transducer with a maximum temperature sensitivity of about −119 • C −1 . The highest magnitudes of temperature sensitivity occurred between +30 • C and +50 • C. Therefore, the ferrite could be sensitive enough to allow temperature measurements at the human body temperature level.The results indicate that the temperature range of maximum temperature sensitivity of the ferrite may be adjusted by means of appropriate selection of the fabrication parameters.
Ni-Co ferrites are magnetostrictive ceramics that have potential application in magnetostrictive/ magnetoelastic sensors, as well as in magnetoelectric composites. Ni-rich Ni-Co spinel ferrite samples were processed by the ceramic method and bulk samples were sintered at 1350 ºC in the solid state and at 950 ºC with Bi2O3 liquid phase. The sintered samples were characterized by light microscopy, scanning electron microscopy, Raman spectroscopy, vibrating sample magnetometry and capacitance dilatometry. With Bi2O3 additions as small as 0.6 mol% it was possible to sinter the Ni-Co ferrite at 950 ºC, obtaining high-density samples; however, such liquid-phase sintered samples presented iron oxide particles. The studied samples presented magnetoelastic sensitivities very close to CoFe2O4, with significantly lower magnetic hysteresis. The results thus indicate that the magnetic properties of the samples analyzed are suitable for applications in magnetomechanical sensors.
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