We report  the influence of different glycine-to-nitrate ratios on the physical and magnetic properties for synthesized zinc-ferrite by  microwave-assisted combustion route. Phase impurity and surface morphology investigated with XRD analysis and field emission- scanning electron microscopy, indicated that  spinel structure  were  formed.Average particles size increased  with the decrease of glycine to nitrate ratio. Magnetic measurement  results indicated that  high values of saturation magnetization  were produced with low  glycine/nitrate ratio. Optical properties of  the investigated ferrites exhibited photo absorption from UV to visible region with  energy gap values that decreased  with the decrease of glycine-to-nitrate ratio. Mainly two broad metal-oxygen bands for zinc-ferrite  were seen in FT-IR spectra.

Mixed spinel Mg1-xZnxFe2O4 ferrites (where x = 0, 0.2, 0.4, and 0.6) nanoparticles were synthesized by using microwave-assisted combustion route. As-synthesized powdered samples were checked by XRD analysis, field emission-scanning electron microscopy, and vibration sample magnetometer to investigate the structural,   morphology, and magnetic properties, respectively. XRD results exhibited that the crystallite size increases with the decrease of Zn+2 ion concentration for series of mixed spinel Mg1-xZnxFe2O4 ferrite expect x=0.2. All the mixed spinel Mg1-xZnxFe2O4 ferrite has different grain sizes with uniform distribution also presence voids in the samples. Pure magnesium ferrite has a lower net magnetization value but when magnesium ions (Mg+2) are replaced by zinc ions (Zn+2) then the value of saturation magnetization increases.

Three samples of spinel powdered zinc ferrites were successfully fabricated via microwave-assisted combustion method followed by calcination at temperature of 500oC for three hours. Phase purity and surface morphology that estimated via XRD pattern and field emission-scanning electron microscopy images (FE-SEM) showed that the samples have cubic spinel - structure with average crystallite size is increase from 15.8 nm to 26.53 nm and from (23.03nm to 28.16 nm when glycine–to-nitrate ratio is decreased before and after calcination at 500 oC for three hours. However the calcination results is increase in average crystallite size and average lattice constant. FE-SEM image indicated that the particles Zinc ferrite possesses shape symmetry and uniformity. Fourier transform infrared spectroscopy (FT-IR) were us to study vibration mode in synthesized spinel ferrite. As calcination the absorption band of a specific bonds are shifted to a lower wavenumber.

In this paper, mixed spinel Co0.4Zn0.6Fe2O4 ferrite was synthesized by microwave-assisted combustion method. Photocatalytic activity of the as-synthesized sample was investigated against methylene blue dye at room temperature at different exposure times (60-360 min.) under visible light. Phase impurity and surface morphology which are investigated with XRD analysis and field emission- scanning electron microscopy, indicate that a cubic spinel unit cell structure with a crystilite size and lattice constant are 22.5048nm and 8.37Å, respectively. The saturation magnetization exhibited directly from the hysteresis loop is (70.20emu/g). Optical properties for the investigated ferrites exhibited photo absorption from UV to visible region with an energy gap of (1.6 eV). Mainly two broad metal-oxygen bands for spinel Co0.4Zn0.6Fe2O4 ferrite  photocatalyst are seen in FT-IR spectra. The degradation ratio of dye increased as exposure time was increased .