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The local atomic arrangements in an Au‐40 at.% Pd alloy were investigated by measuring the X‐ray diffuse scattering from a single crystal. A computer simulation of the short‐range structure was used in the interpretation of the diffuse scattering results. The interpretation indicated a tendency toward the formation of a tetragonal AB long period superlattice which has not previously been observed to occur. The static displacements of the atoms from their average positions were shown to be very small in this alloy.

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Nine new zinc/cadmium-based CPs derived from X-H2BDC (X = H, Br, NO2 and CH3) and methyl-functionalized dmbpy ligands have been prepared. Their luminescent properties and the pH-dependent stabilities in aqueous solutions were investigated.