CaCO 3 nanoparticles with an average size of 45 nm were synthesized via the carbonation method. The tribological properties of the CaCO 3 nanoparticles as an additive in lithium grease were evaluated with a four-ball tester. The results show that these CaCO 3 nanoparticles exhibit good performance in anti-wear and friction-reduction, load-carrying capacity, and extreme pressure properties. The action mechanism was estimated through analysis of the worn surface with X-ray photoelectron spectroscopy (XPS) and scanning electron microscope (SEM). The results indicate that a boundary film mainly composed of CaCO 3 , CaO, iron oxide, and other organic compounds was formed on the worn surface during the friction process.

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