This study was designed to comparative evaluate the chemical composition of the essential oil from twig, leaf and root parts ofClerodendrum inerme(L.)Gaertn. GC-MS analyses of the oils revealed the presence of 8, 8 and 6 compounds in the essential oils obtained by hydrodistillation from different parts, respectively. Higher amounts of esters were found to compose a major chemotype in diverse parts of the plant. Dibutyl phthalate was the main component of all the essential oils attaining in average 34.22%, 59.28% and 44.27% and the other kind of esters accounted for 38.30%, 17.28% and 10.89% in the twig, leaf and root parts, respectively. In addition, some pharmaceutical components such as stigmasterol, linoleic acid and ferruginol were discovered. The study offers theoretic basis for utilization of the traditional folk herbC. inerme.

Volatile constituents were isolated from twig, leaf and root parts of Clerodendrum inerme by ligarine extraction and analyzed by gas chromatography (GC) and gas chromatography/mass spectrometry (GC/MS). There were 6, 12 and 10 volatile constituents identified from different parts, respectively. All the extracts have in common a great percentage of esters (28.59–69.76%) and a high amount of fatty acids (19.27–41.85%), with the exception of the extract from root, which consisted mainly of meroterpene (37.61%). The antioxidant activity by DPPH test was investigated for all the extracts. The root extract exhibited strong antioxidant property with IC50 value of 67.5 μg/ml, about 26% of the potency of known antioxidantα-tocopherol, which probably due to the presence of 6-methylene-3,3-diphenyl-1,4-cyclohexadiene (2.12%). And the characteristic odor of root extract could be attributed to the presence of ferruginol (37.61%) with strong sensory property. The results present here indicated a potential source suitable for using as antioxidant agent and offered theoretic basis for utilization of the traditional folk herb C. inerme.

Abstract. Based on the results of single factor experiments on the extraction of total flavonoids content (TFC) in roots of semi-mangrove plant Clerodendrum inerme(L.) Gaertn., operation conditions were optimized with orthogonal methodology. Four factors were applied to evaluate the extraction yield, including the ethanol concentration, extraction time, temperature and solid to liquid ratio. According to the experimental results, the influence order of different factors on the yield of TFC from the roots: ethanol concentration > solid to liquid ratio > extraction temperature > extraction time. The optimum operating parameters were determined as following, ethanol concentration of 70.0 %, extraction time of 90.0 min, temperature of 60.0 °C and solid to liquid ratio of 1:30. Under the optimized conditions, the maximal yield of TFC was enhanced to 1.279%.

Super-aligned multi-walled carbon nanotube arrays on Si wafer were synthesized by low press chemical vapor deposition. The super-thin multi-walled carbon nanotube films were obtained by a drawing process on the side of the vertically aligned carbon nanotubes. The as-synthesized samples were characterized by scanning electron microscopy and optical microscopy. Terahertz time-domain measurements showed that anisotropic transmission properties were observed. The multi-walled carbon nanotube films with various two-dimensional periods and thicknesses displayed remarkably enhanced transmission at the terahertz range. Comparing experimental results with theoretical calculations revealed that the excitation of surface plasmon polaritons on the carbon nanotubes/Si interface was the key mechanism responsible for the enhanced transmission. The resonance peaks were red shifted with increasing period. In the infrared region, no obvious resonance peaks were observed.