The Shigar valley of northern Pakistan is a well‐known region for holding a variety of gemstones. As the gemstone‐bearing rock, post‐collisional leucogranites, and pegmatites in Shigar valley have been sporadically researched but the detailed and updated timing record along with the source rocks were not adequate. Here, we present comprehensive U(‐Th)Pb ages, mineral, and whole‐rock isotopic analyses to investigate the petrogenetic evolution of these granitoids. The zircon, xenotime, and monazite U(‐Th)–Pb ages show crystallization of leucogranites that spanned as recent as ~7–3 Ma. The REEs with nearly smooth patterns and distinct negative Eu anomalies in all the leucogranites and pegmatites with contrasting negative Eu anomalies illustrate significantly plagioclase fractionation. These leucogranites and pegmatites have high SiO2 content showing peraluminous geochemistry. Zircon Hf isotopic composition of leucogranites, pegmatites and gneisses have εHf(t) values of −28.4 to +7.4, −24.0 to −16.5, and −13.2 to +1.8, respectively, which shows crustal origin along with the probable contamination from Kohistan‐Ladakh Arc at depths. Furthermore, monazite Nd isotopic composition of leucogranites, pegmatites, and gneisses have εNd(t) values of −22.9 to −9.5, −25.1 to −22.8, and −26.3 to −24.8, which seems purely from crustal source. The whole‐rock Sr‐Nd‐Hf isotopic composition shows that leucogranites and gneisses have 87Sr/86Sr(i) values of 0.71603 to 0.92518, εNd(t) values of −22.2 to −2.7, and εHf(t) values of −44.1 to −0.2, respectively, that also confines it to the metapelitic origin. Our results overall reveal that the leucogranites are produced mainly by the partial melting of Dassu felsic gneiss from the Karakoram Metamorphic Complex, showing signatures of the upper crustal rocks of the subducting Indian Plate and hybridized juvenile Asian crust. The input of heat for partial melting is likely to be derived either from the lithospheric mantle which followed the slab break‐off or from shear heating along Main Karakoram Thrust. Furthermore, a leucogranite sample yielded a zircon U–Pb age of 84.9 Ma, and monazite U(‐Th)–Pb age of 10.8 Ma. The in‐situ zircon Hf and monazite Nd isotopes yielded εHf(t) values of +3.6 to +10.7, and εNd(t) values of +1.0 to +2.4, whereas the whole‐rock 87Sr/86Sr(i) value is 0.70522, εNd(t) is +1.1, and εHf(t) is +4.8, respectively, which confirms it to be sourced from the nearby Kohistan‐Ladakh Arc.
Fractional crystallization plays a critical role in generating the differentiated continental crust on Earth. However, whether efficient crystal-melt separation can occur in viscous felsic magmas remains a long-standing debate because of the difficulty in discriminating between differentiated melts and complementary cumulates. Here, we found large (~1 per mil) potassium isotopic variation in 54 strongly peraluminous high-silica (silicon dioxide >70 weight %) leucogranites from the Himalayan orogen, with potassium isotopes correlated with trace elemental proxies (e.g., strontium, rubidium/strontium, and europium anomaly) for plagioclase crystallization. Quantitative modeling requires up to ~60 to 90% fractional crystallization to account for the progressively light potassium isotopic composition of the fractionated leucogranites, while plagioclase accumulation results in enrichment of heavy potassium isotopes in cumulate leucogranites. Our findings strongly support fractional crystallization of high-silica magmas and highlight the great potential of potassium isotopes in studying felsic magma differentiation.
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