The high transparency of carbon-containing materials in the spectral region of "carbon window" (lambda approximately 4.5-5nm) introduces new opportunities for various soft X-ray microscopy applications. The development of efficient multilayer coated X-ray optics operating at the wavelengths of about 4.5nm has stimulated a series of our imaging experiments to study thick biological and synthetic objects. Our experimental set-up consisted of a laser plasma X-ray source generated with the 2nd harmonics of Nd-glass laser, scandium-based thin-film filters, Co/C multilayer mirror and X-ray film UF-4. All soft X-ray images were produced with a single nanosecond exposure and demonstrated appropriate absorption contrast and detector-limited spatial resolution. A special attention was paid to the 3D imaging of thick low-density foam materials to be used in design of laser fusion targets.
We study two C(5 nm)/Co/C(5 nm) multilayer stacks with cobalt layer thicknesses of 4 and 13 nm. Structural analysis of fabricated systems reveals corresponding cobalt layers to be in amorphous (nanocrystalline) and [0001]-textured hcp-phase. The magnetic measurements for both systems agree well with structural data. For the amorphous cobalt layer magnetic data reveal the absence of carbides, high saturation field of 1.6 Â 10 4 Oe and vanishing inplane coercive field. We also show that strong inplane anisotropy can be introduced into the amorphous cobalt film by controlling the process parameters of DC-magnetron sputtering. For the textured hcp-cobalt film we have deduced the presence of randomly close-packed (rcp) structure. We assume this defect-rich cobalt hcp-phase to be responsible for the detected elimination of the out-of-plane magnetic anisotropy in the corresponding multilayer sample.
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