Seventeen ceramics samples (515±95 BP, about 580 years old) and two clay raw materials from Zamala (Far-northern, Cameroon) were characterized by X-ray diffraction (XRD), thermal analysis (DTA/TG) and X-ray fluorescence spectroscopy. The aim of the work was the deduction of the production technology and provenance of these ceramics. With the exception of one sample the analysed ceramics formed a homogeneous chemical and mineralogical group. The observed mineralogical phases were quartz, mica (biotite), potassium feldspar (microcline) and plagioclase (albite and oligoclase). The XRD study of two local clays yielded the presence of quartz, kaolinite, mica, feldspar and plagioclase. The presence of the broad endothermic peak in the DTA/TG curves of the clays and its absence in the curves of the ceramics indicated that the firing temperature of the ceramics was above 550-600 °C, which is the temperature of the kaolinite-metakaolinite transformation. The firing experiments of the clay between 400-1200 °C in oxidizing atmosphere showed that mica disappeared above 900 °C. Therefore, the firing temperature of the sherds should have been between 600-900 °C. The chemical correlation between ceramics and local clay materials pointed out to a local production of these ceramics. Keywords: Zamala, Cameroon, archaeological ceramics, clays, characterization, production technology, provenance. Resumo Dezessete amostras de cerâmica (515±95 AP, cerca de 1435 d.C.) e duas argilas de Zamala (Extremo Norte, Camarões) foram caracterizadas por difração de raios X (DRX), análise térmica (DTA/TG) e espectroscopia de fluorescência de raios X. O objetivo do trabalho foi a dedução da tecnologia de produção e proveniência dessas cerâmicas. Com exceção de uma amostra, as cerâmicas analisadas formaram um grupo químico e mineralógico homogêneo. As fases mineralógicas observadas foram quartzo, mica (biotita), feldspato de potássio (microclínio) e plagioclásio (albita e oligoclásio