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In this work, superparamagnetic Fe3O4@PPy nanocomposite with core‐shell structure having strong near‐infrared (NIR) absorption is synthesized via a facile two‐step modified procedure. The prepared nanocomposite samples are characterized by UV–vis, FTIR, SEM, TEM, VSM, and XRD. The effects of laser power density (1.5–2.5 W cm−2) and aqueous concentration (0.01–0.2 mg ml−1) of the nanocomposite on the photothermal performance are investigated in the NIR region (808 nm). At 0.1 mg ml−1 concentration, the temperature reaches up to 50.1°C, 64.1°C, and 78.4°C within 10 min, under 1.5 W cm−2, 2.0 W cm−2, and 2.5 W cm−2 NIR laser power density values, respectively. Photothermal conservation efficiency is calculated as 43.9% and the nanocomposite exhibits excellent photothermal stability. In summary, the core‐shell Fe3O4@PPy nanocomposite is a promising candidate for photothermal therapy and simultaneous magnetic field‐guided treatments.

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In this study, graphene oxide‐iron oxide‐polypyrrole (GO‐Fe3O4‐PPy) ternary nanocomposites having high photothermal activity and stability are synthesized and analyzed using ultraviolet–visible (UV–Vis) spectroscopy, Fourier transform infrared (FTIR), X‐ray diffraction spectroscopy (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), high‐resolution transmission electron microscopy (HRTEM), and magnetic hysteresis measurement (VSM). The effect of power density (1.5–2.5 W cm−2), concentration (0.01–0.2 mg mL−1), and component composition of nanocomposites on the photothermal properties in the near‐infrared (NIR) region (808 nm) is examined. The results show that superparamagnetic GO‐Fe3O4‐PPy ternary nanocomposite exhibits excellent photothermal performance. The temperature reaches to 55.5, 72.3, and 83.1 °C under the irradiation of the 808 nm NIR laser at 1.5, 2.0—, and 2.5 W cm−2 of power density for 10 min at 0.1 mg mL−1 photothermal therapy (PTT) agent, respectively, and moreover it has excellent photothermal stability. In summary, it is concluded that synthesized nanocomposites potentially may be used in simultaneous magnetic field‐guided treatments. © 2019 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2019, 137, 48837.