Improving the tribological characteristics of water-based drilling fluids by adding graphene-based lubricants has garnered attention because of the potential for a range of inorganic-material-based additives at high temperature. In this study, we constructed a green and simple adsorption approach to prepare highly dispersed graphite using a cationic surfactant for graphite modification. The findings demonstrated that the prepared graphite was highly dispersed in water and had a low sedimentation rate and small contact angle in distilled water. The concentration dosage of cetyltrimethylammonium chloride (CTAC) on graphite was 0.02 g/g. We evaluated the performance of the modified graphite as a lubricated additive in water-based drilling through a rheological study and viscosity coefficient measurement. The results showed that the viscosity coefficient of drilling fluid with 0.05% modified graphite was reduced by 67% at 180 °C. We proved that the modified graphite can significantly improve the lubrication performance of drilling fluid. Furthermore, we revealed the lubrication mechanism by analyzing the chemical structural and crystalline and morphological features of graphite through a particle size test, zeta potential test, Fourier transform infrared (FTIR) spectroscopy, X-ray powder diffraction (XRD), and scanning electron microscopy (SEM) measurements. The results indicated that the modification of graphite by CTAC only occurs through physical adsorption, without changing the crystal structure. These findings provide a reference for the development of high-performance water-based drilling fluids.
According to the conventional well cementing method, the cementing sliding sleeve, as a key part of the casing, needs to be opened by switch tool step by step to conduct fracture with coiled tubing. However, it usually needs switch tool to locate accurately, which is indeed a challenge. This article proposes a set of fracturing sliding sleeve with six-openingdegree and hydraulic switch tool working with coiled tubing-enabled fracturing sliding sleeve. The three-dimensional models, finite element analysis, and flow analysis of the tool are also adopted, which can validate the rationality of the tool's structure. The experimental tests show that the sliding sleeve can be opened or closed with multi-opening degree easily and overcome the gas coning, which can fully meet the requirements of down-hole operation. In addition, the switch tool can open or close the sliding sleeve under lower pressure, and it has a high success rate to open or close the sliding sleeve by coiled tubing without precision location.
In this study, the foaming properties of a compound surfactant formula containing cetyltrimethylammonium chloride (CTAC), cocamidopropyl betaine (CDAB), fatty alcohol polyoxyethylene ether-7 (AEO7) and sodium alpha-olefin sulfonate (AOST) were evaluated to meet the application requirements for foam generation and foam drainage in gas wells. The results exhibited that the foaming volume and the half-life of the compound surfactant solution (0.05 wt % CTAC + 0.7 wt % CDAB + 0.6 wt % AEO7 + 0.05 wt % AOST) can reach the values of 550 mL and 23 min, respectively, which suggested that the foaming ability and stability were improved in comparison with each solution containing a single surfactant. It showed that the surface tension can be lowered to 22.4 mN/m with the presence of the compound surfactants. Simultaneously, the microstructure of the foam was observed using a polarizing microscope, and it was found that there were almost no polyhedron structures in the foam within a certain range of formula concentrations. The results of the experiments also clarify that the formula has well properties of temperature resistance and salt resistance (measured using a high-speed agitator).
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