Научно-исследовательский физико-технический институт Нижегородского государственного университета им. Н.И. Лобачевского, 603950 Нижний Новгород, Россия * Нижегородский государственный университет им. Н.И. Лобачевского (физический факультет),

The results of studying GaInAs/GaInP/GaAs photodiode structures grown by metal–organic vapor-phase epitaxy are reported. A procedure for the diagnostics of such multilayer structures is developed. The procedure is based on the application of Raman spectroscopy in combination with photoluminescence spectroscopy in the mode of the lateral scanning of transverse cleavages. The compositions of the GaInAs and GaInP solid solutions are determined.