A series of novel carbamate compounds were obtained from one pot three component reaction of aldehydes, bromohydrocarbons and isocyanates mediated by zinc powder under room temperature. This protocol has advantages of mild conditions, simple work-up, high yield, easily available starting materials and fast reaction rate. The structures of all products were characterized by 1 H NMR, 13 C NMR, IR, HRMS and elemental analysis.
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