In this study, dye encapsulated microcapsules were produced by polyurethane prepolymer synthesis method using hexamethylene diisocyanate, ethylene glycol and methyl ethyl ketone. The study showed that the average size of microcapsules were 4.697 in normal distribution. These microcapsules were induced red color by thermochromic fluoran red ㎛ dye with showing color change as temperature. After the textile finishing of microcapsules, durability of microcapsules were checked as crocking times and lightfastness. The microcapsules were pressed at protrusion of textile weave in 10 crocking times which meant that the microcapsules not fallen off. Lightfastness was acceptable giving rating 4. It means that the polyurethane microcapsules not affect to light durability.
In this study, dye-encapsulated microcapsules were produced by emulsion polymerization using styrene monomer. The study showed that the average size of microcapsules were 2~5㎛ in normal distribution. These microcapsules induced pale yellow(A12) and reddish yellow(B24) color by thermochromic fluoran yellow(dye A) and red(dye B). These microcapsules were changed to dark yellow(A12) and scarlet(B24) color depending on temperature change. The weight of microcapsules decreased by 7% to 11% during the heating ranges from 320℃ to 350℃ implying that the styrene microcapsules had thermal stability upto 300℃.
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