A model investigation of the effect of plasticizer on radiation stability of poly(vinyl chloride)

Szymański, W.; S̀mietańska, G.; Truszkowski, S.

doi:10.1002/pol.1980.130181208

J. Polym. Sci. B Polym. Lett. Ed.

1980

DOI: 10.1002/pol.1980.130181208

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A model investigation of the effect of plasticizer on radiation stability of poly(vinyl chloride)

W. Szymański¹,

G. S̀mietańska²,

S. Truszkowski³

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1982

1986

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Cited by 2 publications

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Degradation studies of plasticized PVC. I. Multiple internal reflection infrared spectroscopy

Hill

1982

J of Applied Polymer Sci

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SynopsisMultiple internal reflection infrared spectroscopy (MIR) was used to study surface degradation in commercial and laboratory prepared plasticized PVC samples. Samples were subjected to accelerated (W exposure) and natural weathering. Ultraviolet-exposed samples show peak formation at 3200 cm-l (OH), and 1400 cm-1 (CH bend), as well as increased absorption at 1720 cm-1 (CO).Outdoor-exposed samples show essentially similar changes, but the variation in peak ratio shows large variations of a random nature; it has been proposed that rainfall has a major influence on surface plasticizer concentration.

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Degradation studies of plasticized PVC. I. Multiple internal reflection infrared spectroscopy

Hill

1982

J of Applied Polymer Sci

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Radiolysis of aliphatic chlorohydrocarbons: I. radiation yield of stable products of radiolysis of 1,4-dichlorobutane and 1,4-dichlorobutane-2 gamma-irradiated in an oxygen-free atmosphere

Szymański¹,

Mietańska²,

Kowal³

1986

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The stable products of radiolysis of 1,4-dichlorobutane (1,4-DCB) and 1,4-dichlorobutene-2 (1,4-DCB-2) gamma-irradiated in an oxygen-free atmosphere were investigated. The pure products of radiolysis were separated by preparative gas chromatography and identified by N MR and mass spectroscopy as well as qualitative gas chromatography. The compounds formed were determined by potentiometric analysis and quantitative gas chromatography. From the 1,4-DCB we have obtained in the gas phase: HCI, CHsCI, 1-chlorobutane and the 1,3-and 1,4-isomers of dichlorobutane; in the liquid phase: 1,3-dichlorobutane, 1,1,4-and 1,2,4-isomers of trichlorobutane, the dimer and trimer of the initial compound. From the 1,4-DCB-2 we have found in the gas phase: HCI and cis, trans-isomers of the initial compound; in the liquid phase: 3,4-dichlorobutene-1, 1,2,4-trichlorobutane and a mixture of the oligomers of 1,4-DCB-2 (dimer and trimer). On the basis of the results obtained a preliminary scheme for the formation of the stable products is proposed.

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A model investigation of the effect of plasticizer on radiation stability of poly(vinyl chloride)

Cited by 2 publications

References 9 publications

Degradation studies of plasticized PVC. I. Multiple internal reflection infrared spectroscopy

Degradation studies of plasticized PVC. I. Multiple internal reflection infrared spectroscopy

Radiolysis of aliphatic chlorohydrocarbons: I. radiation yield of stable products of radiolysis of 1,4-dichlorobutane and 1,4-dichlorobutane-2 gamma-irradiated in an oxygen-free atmosphere

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