2022
DOI: 10.22159/ijap.2022v14i4.44774
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A New Stability Indicating Uplc Method for the Determination of Two Antidiabetic Drugs in Combination: Applications to Bulk and Tablet Formulation

Abstract: Objective: This work was intended to develop a rapid and sensitive stability-indicating ultra-performance liquid chromatographic (UPLC) method for the determination of Metformin and Gliclazide simultaneously in their pharmaceutical bulk and tablet formulation. Methods: Separation was performed on Lunna C18 (100 mm x 2.6 mm, 1.6µ) column by using trifluoroacetic acid buffer: acetonitrile (70: 30, v/v) as a mobile phase at a flow rate of 1 ml/min and a wavelength of detection of 227 nm. Method validation and for… Show more

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