1949
DOI: 10.1021/ja01173a057
|View full text |Cite
|
Sign up to set email alerts
|

A Novel Sulfidation Reaction and its Application to Some 4-Substituted-2-aminothiazoles

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...
2
1
1
1

Citation Types

0
7
0

Year Published

1979
1979
2016
2016

Publication Types

Select...
5
1

Relationship

0
6

Authors

Journals

citations
Cited by 16 publications
(7 citation statements)
references
References 0 publications
0
7
0
Order By: Relevance
“…5,5′‐Thiobis(2‐amino‐4‐methyl‐thiazole) (DA) was synthesized in our laboratory according to the reported procedure,43 and recrystallized twice from ethanol. Triphenyl phosphite (TPP, MERCK, Schuchardt, Germany) and trimellitic anhydride (TMA, MERCK, Schuchardt, Germany) were used without further purification.…”
Section: Methodsmentioning
confidence: 99%
“…5,5′‐Thiobis(2‐amino‐4‐methyl‐thiazole) (DA) was synthesized in our laboratory according to the reported procedure,43 and recrystallized twice from ethanol. Triphenyl phosphite (TPP, MERCK, Schuchardt, Germany) and trimellitic anhydride (TMA, MERCK, Schuchardt, Germany) were used without further purification.…”
Section: Methodsmentioning
confidence: 99%
“…The diamines ( Ia , Ib ) were obtained from condensation of thiazoles with formaldehyde or thiourea [36, 38] which upon reaction with chloroacetyl chloride at room temperature led to dichlorodiamides ( IIa , IIb ) in 2 h. The dichloro compounds ( IIa , IIb ) easily reacted with dithioate salts at room temperature and produced the podands Va , Vb , Vc , Vd , Ve , Vf (Scheme and Table ).…”
Section: Resultsmentioning
confidence: 99%
“…A novel diamine monomer, 5,5′‐thiobis(2‐amino‐4‐phenylthiazole) (DA), was synthesized in our laboratory according to a modified reported procedure …”
Section: Methodsmentioning
confidence: 99%
“…A novel diamine monomer, 5,5 ′ -thiobis(2-amino-4-phenylthiazole) (DA), was synthesized in our laboratory according to a modified reported procedure. 23 N-methyl-2-pyrrolidone (NMP; Merck) and pyridine (Py; Fluka) were purified by distillation under reduced pressure over calcium hydride prior to use. LiCl (Merck) was dried for 24 h at 180 ∘ C under vacuum before use.…”
Section: Experimental Materialsmentioning
confidence: 99%