2009
DOI: 10.1107/s0108270109027735
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A novel trinuclear zinc(II) cluster with a tetrahedral ZnO4core

Abstract: The reaction of 0.67 molar equivalents of the O,N,O'-tridentate zwitterionic Schiff base (2Z,4E)-4-[(2-hydroxyphenyl)iminio]pent-2-en-2-olate (H2L) with one equivalent of zinc(II) acetate in methanol affords a novel trinuclear Zn(II) cluster, di-mu-acetato-1:2kappa2O:O';2:3kappa2O:O'-dimethanol-1kappaO,3kappaO-bis{mu-2-[(2E,3Z)-4-oxidopent-3-en-2-ylideneamino]phenolato}-1:2kappa4O2,N,O4:O4;2:3kappa4O4:O2,N,O4-trizinc(II), [Zn3(C11H11NO2)2(C2H3O2)2(CH4O)2], (I), in which two bridging acetate ligands link the te… Show more

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Cited by 3 publications
(2 citation statements)
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“…For the structures of zinc complexes with Schiff base ligands, see: Munro et al (2009); Granifo et al (2006). For a monoclinic polymorph of the title compound in the space group P2 1 /n, see: Han et al (2010).…”
Section: Related Literaturementioning
confidence: 99%
See 1 more Smart Citation
“…For the structures of zinc complexes with Schiff base ligands, see: Munro et al (2009); Granifo et al (2006). For a monoclinic polymorph of the title compound in the space group P2 1 /n, see: Han et al (2010).…”
Section: Related Literaturementioning
confidence: 99%
“…Data collection: SMART (Bruker, 2001); cell refinement: SAINT (Bruker, 2001); data reduction: SAINT; program(s) used to solve structure: SHELXTL (Sheldrick, 2008); program(s) used to refine structure: SHELXTL; molecular graphics: SHELXTL; software used to prepare material for publication: SHELXTL and local programs. The structures of zinc complexes with Schiff bases have received a great deal of attention (Munro et al, 2009;Granifo et al, 2006). The title compound was first reported in the monoclinic space group P2 1 /n (Han et al, 2010).…”
Section: Data Collectionmentioning
confidence: 99%