A Review on Solid Phase Micro Extraction—High Performance Liquid Chromatography (SPME-HPLC) Analysis of Pesticides

Aulakh, Jatinder Singh; Malik, Ashok Kumar; Kaur, Varinder; Schmitt‐Kopplin, Philippe

doi:10.1080/10408340590947952

Cited by 175 publications

(97 citation statements)

References 44 publications

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“…Today, there are also many applications in the biomedical field [245] and for food analysis [246]. Moreover, as was discussed above, the technique is also used for less volatile compounds [234].…”

Section: Solid-phase Micro-extractionmentioning

confidence: 99%

Modern Methods of Sample Preparation for GC Analysis

Koning¹,

Janssen

Brinkman

2009

Chroma

122

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Today, a wide variety of techniques is available for the preparation of (semi-) solid, liquid and gaseous samples, prior to their instrumental analysis by means of capillary gas chromatography (GC) or, increasingly, comprehensive two-dimensional GC (GC 9 GC). In the past two decades, a large number of 'modern' sample-preparation techniques has been introduced, which have partly superseded their 'classical' counterparts. These novel techniques include off-line and on-line (sometimes semi-or fully automated) procedures, and exhaustive extraction as well as equilibrium techniques. In order to improve overall performance, aspects such as essentially organic solvent-less approaches, large-volume injection and miniaturization receive increasing attention. In most recent applications, mass spectrometric or element-selective detection have been used. The present review discusses the advantages and disadvantages, and relative performance, of most of the modern samplepreparation techniques and cites a number of illustrative applications for each of them.

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Section: Solid-phase Micro-extractionmentioning

confidence: 99%

Modern Methods of Sample Preparation for GC Analysis

Koning¹,

Janssen

Brinkman

2009

Chroma

122

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“…Richard [10] employed HPLC method to determine carbamate residues using post-column hydrolysis electrochemical detection. Aulakh et al [11] reported solid phase microextraction HPLC for the analysis of pesticides. Tomomi et al [12] developed a new analytical method for the determination of nine pesticide residues including chlorpropham in fruits and vegetables using ESI-LC/MS/MS with direct sample injection into a short column.…”

Section: Chlorpropham (C 10 H 12 Clno 2 )mentioning

confidence: 99%

Comparative voltammetric study and determination of carbamate pesticide residues in soil at carbon nanotubes paste electrodes

Babu¹,

Reddy²,

P.Sujana³

2014

J. Electrochem. Sci. Eng.

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“…High-performance liquid chromatography (HPLC) is preferred with various detection systems including ultraviolet (UV) [20][21][22][23], diode array detection (DAD) [23][24][25][26], MS [27,28] and tandem mass spectrometry (MS n ) [29], and fluorescence detection (FLD) [30]. Generally, LC-MS techniques are considered superior to all the above-mentioned detection techniques, in terms of specificity and sensitivity.…”

Section: Introductionmentioning

confidence: 99%

Determination of Deltamethrin in Mice Plasma and Immune Organs by Simple Reversed-Phase HPLC

Kumar¹,

Dubey²,

Kant³

et al. 2016

Acta Chromatographica

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Deltamethrin, a well-known type 2 synthetic pyrethroid insecticide, is a widespread environmental toxicant. It has potential to accumulate in body fluids and tissues due to its lipophilic characteristics. The immune system is among the most sensitive targets regarding toxicity of environmental pollutants. Various methods are available in the literature to analyze deltamethrin (DLM) concentration in plasma and tissues, but regarding the immune organs, only one gas chromatography–tandem mass spectrometry (GC–MS/MS) method (on spleen tissues) has been reported. In the present investigation, a rapid and sensitive high-performance liquid chromatography (HPLC) method has been developed and validated to determine DLM concentration in plasma, thymus, and spleen using zaleplone as an internal standard. Liquid chromatography (LC) separation is performed on an Agilent Zorbax® C8 column (250 mm × 4.6 mm, i.d., 5 μm) with isocratic elution using a mobile phase consisting of acetonitrile–5 mM KH2PO4 (70:30, v/v) at a flow rate of 1 mL min−1. The lower limit of quantification (LLOQ) for DLM is 10 ng mL−1 (plasma, thymus, and spleen). The method has been validated in terms of establishing linearity, specificity, sensitivity, recovery, accuracy, and precision (intra- and inter-day) and stabilities study. This validated method was successfully applied to a pharmacokinetic and tissue distribution study of DLM in mice.

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A Review on Solid Phase Micro Extraction—High Performance Liquid Chromatography (SPME-HPLC) Analysis of Pesticides

Cited by 175 publications

References 44 publications

Modern Methods of Sample Preparation for GC Analysis

Modern Methods of Sample Preparation for GC Analysis

Comparative voltammetric study and determination of carbamate pesticide residues in soil at carbon nanotubes paste electrodes

Determination of Deltamethrin in Mice Plasma and Immune Organs by Simple Reversed-Phase HPLC

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