Despite having a population of 16.3 million, Kinshasa, Democratic Republic of the Congo (DRC), has had little attention toward air quality monitoring. We deployed a MetOne Beta Attenuation Monitor (BAM-1020) for reference PM 2.5 and a QuantAQ Modulair, the latter of which includes measurements of gas-phase NO 2 , O 3 , CO, and CO 2 , in addition to PM 1 , PM 2.5 , and PM 10 . Here we present the first results from this aggregated, multisensor, multispecies network in DRC. We first compare the Modulair against the BAM-1020, finding an r 2 of 0.76 and a mean absolute error (MAE) of 6.97 μg m −3 (hourly data). We develop a correction factor using multiple linear regression, improving MAE to 5.54 μg m −3 . We leverage gaseous pollutant concentrations, particle size distribution data, and anemometer data to draw conclusions about the sources of PM 2.5 in Kinshasa. We link factors resolved from a non-negative matrix factorization method using the gaseous and particle bin concentrations to source profiles. We find a 3-factor solution that points to a COdominated, supermicron particle source indicative of secondary particles from local combustion, along with a submicron particledominated source indicative of primary particles from combustion and a regional biomass burning source. Our results highlight the need for the implementation of clean air solutions in the DRC.