Acoust ic rhinometry allows an objective and non-invasive assessment of nasal geometry. Aim: The present study aimed at determining the volumes of specific segments of the nasal cavity in healthy adults including the nasopharynx, using acoustic rhinometry. Study design: A clinical prospective analysis. Cases and Method: Thirty volunteers with no evidence of nasal obstruction, aged 18 to 30 years (14 males and 16 females) were analyzed. Volumes were measured at the nasal valve region (V 1 ), the turbinates (V 2 ), and the nasopharynx (V 3 ), before and after application of a topical nasal vasoconstrictor. Results: The mean volumes measured in 60 cavities before nasal decongestion, were: 1.81±0.35cm 3 (V 1 ), 4.02±1.41cm 3 (V 2 ), and 17.52±4.44cm 3 (V 3 ) for males, and 1.58±0.25cm 3 (V 1 ), 3.94±1.03cm 3 (V 2 ), and 17.80±2.73cm 3 (V 3 ) for females. Gender differences were only significant in V 1 (p<0.05). After nasal decongestion, the volumes of all the analyzed segments were significantly larger (p<0.05), and the gender differences were significant for V 1 and V 2 . Conclusion: Volumes of the three segments in adults with no evidence of nasal obstruction may be used as reference values for other studies.