A study of some gases emitted from three industries at Ama industrial complex, Nigeria, was carried out using Crowcon Gasman, single gas monitors. Results showed that HCN (0.94 ± 0.16 ppm) and CO (3.17 ± 0.89 ppm) emissions from Brewery were significantly (P < 0.05) higher than those of Bottling Company A (0.46 ± 0.12 and 0.65 ± 0.10 ppm, respectively). NH 3 , SO 2 and NO 2 emissions were the same. Cl 2 emissions from Bottling Company A and Bottling Company B were the same, but each was significantly (P < 0.05) higher than that of Brewery. H 2 S emission from Bottling Company A (21.24 ± 0.97 ppm) was significantly (P < 0. 05) higher than that from Brewery (17.71 ± 0.94 ppm), which was significantly higher than that of Bottling Company B (12.57 ± 0.32 ppm). Apart from CO and NH 3, the concentrations of other gaseous emissions exceeded the Nigerian and United States national ambient air quality standards. Therefore, it is recommended that these companies should determine appropriate control measures to reduce these toxic emissions.