2017
DOI: 10.1016/j.actamat.2016.11.053
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An Atom Probe Tomography study of site preference and partitioning in a nickel-based superalloy

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Cited by 130 publications
(52 citation statements)
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“…Besides, C and Si were found to segregate to the grain boundary up to 0.5 and 0.2 at.%, respectively, but no specific role on the hot cracking was observed from their presence at the grain boundary. The segregation behavior observed here is in agreement with previous reports [26,32,33]. Segregation of Zr and Hf at the grain boundary was not observed, instead they were found to partition within the γ', as shown in Supplementary Figure 1(a).…”
Section: Microstructural Characterization: Cracked Columnar Samplesupporting
confidence: 93%
“…Besides, C and Si were found to segregate to the grain boundary up to 0.5 and 0.2 at.%, respectively, but no specific role on the hot cracking was observed from their presence at the grain boundary. The segregation behavior observed here is in agreement with previous reports [26,32,33]. Segregation of Zr and Hf at the grain boundary was not observed, instead they were found to partition within the γ', as shown in Supplementary Figure 1(a).…”
Section: Microstructural Characterization: Cracked Columnar Samplesupporting
confidence: 93%
“…APT analysis revealed that these borides are mainly Cr-rich whereas W and Mo contribute in lower amounts, as shown in at.%. A similar observation was previously reported regarding the composition of these secondary precipitates from an APT analysis of a powder nickel-based superalloy [38].…”
Section: Primary Grain Boundary Phases After Heat Treatmentsupporting
confidence: 88%
“…A similar effect was observed for Ti, Ta, and Hf in the RR1000 alloy as seen by Bagot et al, [40] where it was attributed to the large lattice misfits for these elements as estimated using Vegard's Law. [1] Cr concentration profiles were also found to be non-uniform heading into the c matrix phase, showing a trend of rising to a plateau concentration of roughly 30 at.…”
Section: B Interface Chemistrysupporting
confidence: 65%
“…However, this study has shown that careful, methodical use of APT can play a key role in benchmarking the results from theoretical predictions, as also recently demonstrated on in-service alloys. [40] This combination of APT and modeling thus offers a robust, general methodology which should be considered in alloy design.…”
Section: Alloy Composition/phase Chemistrymentioning
confidence: 99%