2004
DOI: 10.1520/jfs2002151
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Analysis of Dyes in Illicit Pills (Amphetamine and Derivatives)

Abstract: The determination of dyes present in illicit pills is shown to be useful and easy-to-get information in strategic and tactical drug intelligence. An analytical strategy including solid-phase extraction (SPE) thin-layer chromatography (TLC) and capillary zone electrophoresis equipped with a diode array detector (CZE-DAD) was developed to identify and quantify 14 hydrosoluble, acidic, synthetic food dyes allowed in the European Community. Indeed, these may be the most susceptible dyes to be found in illicit pill… Show more

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Cited by 20 publications
(17 citation statements)
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“…In the past, for both qualitative and quantitative determination techniques such as paper and thin-layer chromatography (Griffiths 1966;Goldmann et al 2004), column chromatography (Patel et al 1986), titration (Ashkenazi et al 1991), electrophoresis (Yeh 1977), spectrophotometry (Prado et al 2006;Graichen 1975) and high-performance liquid chromatography (HPLC) (Yoshioka and Ichihashi 2008) were adopted. We report here a new polyoxometalate cluster, Ln-POM, and its nanohybrid composite with carbon nano-onion.…”
Section: Resultsmentioning
confidence: 99%
“…In the past, for both qualitative and quantitative determination techniques such as paper and thin-layer chromatography (Griffiths 1966;Goldmann et al 2004), column chromatography (Patel et al 1986), titration (Ashkenazi et al 1991), electrophoresis (Yeh 1977), spectrophotometry (Prado et al 2006;Graichen 1975) and high-performance liquid chromatography (HPLC) (Yoshioka and Ichihashi 2008) were adopted. We report here a new polyoxometalate cluster, Ln-POM, and its nanohybrid composite with carbon nano-onion.…”
Section: Resultsmentioning
confidence: 99%
“…The utility of a Bayesian approach in forensic science, including ballistic (Bunch, 2000) and paint matching (McDermott et al, 1999), drug sampling and analysis (Coulson et al, 2001;Goldmann et al, 2004), and DNA identification (Krawczak and Schmidtke, 1992;Evett and Weir, 1998;Thompson et al, 2003;Foreman et al, 1999), is widely known, as it provides the examiner with the likelihood ratio of a positive identification or match that can be presented in court.…”
Section: Osteological Data Likelihood Ratios and Personal Identificmentioning
confidence: 99%
“…The analytical method was based on a buffer containing 20 mM sodium hydrogen phosphate and 10 mM sodium hydrogen carbonate adjusted at pH 10.5 with 0.1 M NaOH. Ten millimolar hydroxypropylb-CD was added together with 4.75% ACN [19]. The separation was performed under 25 kV voltage.…”
Section: Forensic Drugs and Poisonsmentioning
confidence: 99%