Analysis of Physicochemical Properties of W1.8507 Steel Parts with Sharp Edges, Thermochemically Treated by Plasma Nitriding with and without Polarized Screens

Abstract

The plasma nitriding edge effect phenomenon is characteristic of parts with sharp edges. The intersection for the discharge of negative light of the two adjacent faces causes the apparition of this effect. In some cases, this effect causes disturbance to the general process. In this work, a sample with different angles of 30°, 60°, and 90° was analyzed. The sample was subjected to ion nitriding with and without the cathode grid to highlight the reduction of the edge effect on the non-uniformity appearing on the edges and corners of the parts. The effect of the active screen was also analyzed by hardness measurements in the area of the nitride edges and by SEM and EDX analyses in the mentioned areas. Additionally, the influence of active screens was studied by nanoindentation and scratch tests and by measuring the contact angle of coolants and liquid lubricants on the nitride surfaces with both methods.

Ca–Zn Phosphate Conversion Coatings Deposited on Ti6Al4V for Medical Applications

“…For each liquid sample, measurements were carried out at least five times. The average of all the individual measurements was used to compute the contact angle value [33]. Additionally, the Owens-Wendt-Rabel-Kaelble (OWRK) method [34] based on contact angle was used to calculate the sample's surface energy.…”