2013
DOI: 10.1246/cl.130152
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Analysis of Reduced Graphene Oxides by X-ray Photoelectron Spectroscopy and Electrochemical Capacitance

Abstract: Reduced graphene oxide (rGO) and reduced graphite oxide (rGtO) were analyzed by X-ray photoelectron spectroscopy. rGO and rGtO were prepared by photochemical, electrochemical, hydrazine-assisted, and thermal reduction of graphene oxide (GO) and graphite oxide (GtO). The number of CH defects increased for the photochemical and electrochemical reduction, whereas a direct increase in the number of C=C bonds was observed for thermal and hydrazine-assisted reduction. Cyclic voltammograms showed that the electrochem… Show more

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Cited by 112 publications
(83 citation statements)
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“…Figure shows the XPS spectra of C 1s, O 1s, and N 1s in BGOs‐fd and BGOs‐fd‐1000. A typical C 1s and O 1s XPS spectra for GO were obtained for BGOs‐fd, which consisted of peaks assigned to an aromatic and aliphatic carbon at 284.6 eV, and carbon and oxygen atoms in an ether oxygen or hydroxylic group at 286.4 and 532.3 eV, respectively . The presence of residual nitrogen in an amine form was shown by the N 1s XPS spectrum of BGOs‐fd .…”
Section: Resultsmentioning
confidence: 99%
“…Figure shows the XPS spectra of C 1s, O 1s, and N 1s in BGOs‐fd and BGOs‐fd‐1000. A typical C 1s and O 1s XPS spectra for GO were obtained for BGOs‐fd, which consisted of peaks assigned to an aromatic and aliphatic carbon at 284.6 eV, and carbon and oxygen atoms in an ether oxygen or hydroxylic group at 286.4 and 532.3 eV, respectively . The presence of residual nitrogen in an amine form was shown by the N 1s XPS spectrum of BGOs‐fd .…”
Section: Resultsmentioning
confidence: 99%
“…However, deconvolution of this peak is essential for understanding the C1s XPS spectra of GO 35 . This is because the full width at half maximum (FWHM) is too large to assign the band to a single component (1 .3 eV) for GO, considering much smaller FWHM of the C=C peak from highly ordered pyrolytic graphite (0.8 eV) measured with the same experimental conditions 36 .…”
Section: Structural Analysis Of Photoreduced Gomentioning
confidence: 99%
“…Therefore, recently, we have developed deconvolution of C1s XPS spectra in order to identify chemical states of GO, using reference samples with specific oxygen function group (OFG), C-H, C-C, or C=C bonding states 36,37 . In particular, our approach allows for the deconvolution of the peak at ca.…”
Section: Structural Analysis Of Photoreduced Gomentioning
confidence: 99%
“…For the C 1 s spectra of the three GN composites, the peak intensities of the carbons with oxygen-containing groups (HO-C = O, C = O and C-OH) are very low, while those of C = C are considerably high, indicating the effective reduction of the three composites31. There is a very small fitting peak located at 284.0 eV which is assigned to the carbon of carbide nickel32, demonstrating the formation of C-Ni bond.…”
Section: Resultsmentioning
confidence: 98%