Analytical strategies to determine antibiotic residues in fish

Samanidou, Victoria F.; Evaggelopoulou, Evaggelia N.

doi:10.1002/jssc.200700252

Cited by 95 publications

(54 citation statements)

References 59 publications

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“…The accelerated growth of aquaculture has resulted in a series of harmful effects to human health. The widespread and unrestricted use of antibiotics in this industry, to prevent bacterial infections [7], has leaded some excess amount of unutilized antibiotics to remain in the environment. The use of antibiotics and drugs in fish farms has prompted an investigation into the elimination of these residues from fish muscle [8].…”

Section: Introductionmentioning

confidence: 99%

A Review of Antibiotic Residue Determination in Aquatic Products

Mo¹,

Huang²,

Mingxing³

et al. 2017

Proceedings of the 2017 International Conference on Material Science, Energy and Environmental Engineering (MSEEE 2017)

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Abstract. In recent years, with the development of fisheries, the aquaculture industry has developed rapidly and has become an important part of our country economy. At the same time more and more aquatic products is being used by people while the abuse of antibiotics is growing uncontrolled. This paper summarizes the detection methods of various kinds of antibiotics in aquatic products, as well as the method of spiked recovery, detection limit, quantitative limit, and puts forward the corresponding countermeasures proposal of controlling the abuse of antibiotics.

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Section: Introductionmentioning

confidence: 99%

A Review of Antibiotic Residue Determination in Aquatic Products

Mo¹,

Huang²,

Mingxing³

et al. 2017

Proceedings of the 2017 International Conference on Material Science, Energy and Environmental Engineering (MSEEE 2017)

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“…Besides the use of antibiotics as bacterial infection treatment, sulfonamides, β-lactams and macrolides can be used as growth-promoting or infection-preventing agents. They are used in sub-therapeutic doses in animal feed or veterinary drugs [6][7][8][9].…”

Section: Introductionmentioning

confidence: 99%

On the Extraction of Antibiotics from Shrimps Prior to Chromatographic Analysis

et al. 2016

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Abstract:The widespread use of antibiotics in veterinary practice and aquaculture has led to the increase of antimicrobial resistance in food-borne pathogens that may be transferred to humans. Global concern is reflected in the regulations from different agencies that have set maximum permitted residue limits on antibiotics in different food matrices of animal origin. Sensitive and selective methods are required to monitor residue levels in aquaculture species for routine regulatory analysis. Since sample preparation is the most important step, several extraction methods have been developed. In this review, we aim to summarize the trends in extraction of several antibiotics classes from shrimps and give a comparison of performance characteristics in the different approaches.

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“…Tetracyclines are photosensitive; when used as bath solutions for treatment, they decompose and turn brown. This form could be toxic for humans and animals (Samanidou and Evaggelopoulou 2007).…”

Section: Introductionmentioning

confidence: 99%

Investigation of tetracycline residues in fish caught from surrounding fish farms in Mugla district

Türk¹,

Oguz²

2016

EurasianJVetSci

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ÖzAmaç: Su ürünlerindeki ilaç ve metabolitlerinin kalıntı analizleri Ulusal Kalıntı İzleme Planı kapsamında düzenli olarak yapılmaktadır. Fakat Türkiye'de bu kalıntıların sucul ortama etkilerine yönelik araştırmalar sınırlıdır. Bu çalışmada, Muğla bölgesindeki balık çiftliklerinin etrafından avlanan balıklarda tetrasiklin grubu antibiyotiklerin (oksitetrasiklin, tetrasiklin, klortetrasiklin, doksisiklin) kalıntılarının belirlenmesi amaçlandı. Gereç ve Yöntem:Analiz için 70 ayrı çiftlik etrafından toplanan 70 adet balık örneği kullanıldı. Balıklarda tetrasiklin kalıntıları LC MS/MS yöntemi ile analiz edildi. Seçicilik, doğ-rusallık, geri kazanım, duyarlılık ve kesinlik ölçütlerinde metot validasyonu yapıldı. Bulgular:Analizin geri kazanımları oksitetrasiklin için %100.5, tetrasiklin için %101.3, klortetrasiklin için %99 ve doksisilin için %100.5 olarak belirlendi. Analizlerin sonucunda balık örneklerinin hiçbirinde tetrasiklin grubu antibiyotikler tespit edilemedi.Öneri: Yapılan analizlerde balık örneklerinde hesaplanabilir limitlerde tetrasiklin kalıntısı bulunmaması çevre ve halk sağlığı açısından memnuniyet verici olarak kabul edilebilir. Anahtar kelimeler: Balık, tetrasiklin, kalıntı, LC MS/MS AbstractAim: Residue analyses of drugs and metabolites in the aquaculture are regularly conducted under the National Residue Monitoring Plan in Turkey. However, the research on the impact of these residues on the aquatic environment is limited. In this study, it was aimed to analyze the residues of tetracycline group antibiotics in fishes caught around fish farms in the Muğla district. Materials and Methods:Seventy fish samples collected from the vicinity of 70 different fish farms were used for analysis. Tetracycline residues in the fish were analyzed with the LC MS/MS method. Validation was performed with the criteria of specificity, linearity, recovery, precision and sensitivity.Results: Recovery values were determined as follows: Oxytetracycline 100.5%, tetracycline 101.3%, chlortetracycline 99%, and doxycycline 100.5%. At the end of the analyses, no tetracycline antibiotic residues were found. Conclusion:It can be expressed that no tetracycline residues were detected in the samples at the detectable limits is a satisfactory result in terms of public health and environment.

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Analytical strategies to determine antibiotic residues in fish

Cited by 95 publications

References 59 publications

A Review of Antibiotic Residue Determination in Aquatic Products

A Review of Antibiotic Residue Determination in Aquatic Products

On the Extraction of Antibiotics from Shrimps Prior to Chromatographic Analysis

Investigation of tetracycline residues in fish caught from surrounding fish farms in Mugla district

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