Ni diffusion in sub-lOO nm devices can adversely affect electrical performance, and contribute greatly to yield loss. Despite the tremendous advantages of Ni salicide technology over Ti or Co, there are problems associated with the intrinsic properties of NiSi. Ni spiking into Si substrate or conductive bridges between silicide on the gate electrodes and that on the source/drain terminals can occur. These effects can be induced or enhanced by stringent layout, stress or process conditions. Its impact can be evident from electrical failure analysis such as nanoprobing and C-AFM, that are useful in identifying the cause of failure.