In-situ laser-absorption measurements of CO, CO 2 , CH 4 and H 2 O were demonstrated in the synthesis gas products of coal gasification (here called syngas) from an engineering-scale transport reactor. A wavelength-scanned, wavelength-modulation spectroscopy scheme was used to counter environmental challenges including severe loss in transmitted light intensity due to particulate scattering and beam steering in the synthesis gas stream. Separate lasers were used for each species (CO near 2326nm, CO 2 near 2017nm, CH 4 near 2290nm, and H 2 O near 1352nm) and a novel fiber bundle was utilized to combine all four beams on a common optical path. Line-of-sight laser absorption utilized sapphire windows in the synthesis gas product pipe downstream of the gasifier reactor by approximately 5 seconds flow time. Time multiplexing enabled low-noise measurement of the transmitted light with a single detector. Successful measurements of the four species mole fractions were performed throughout the 54 day measurement campaign, including a significant period of unattended operation. The mole fractions of the