2004
DOI: 10.1002/chem.200400451
|View full text |Cite
|
Sign up to set email alerts
|

Atmospheric Pressure Chemical Vapor Deposition: An Alternative Route to Large‐Scale MoS2 and WS2 Inorganic Fullerene‐like Nanostructures and Nanoflowers

Abstract: Large-scale MoS2 and WS2 inorganic fullerene-like (IF) nanostructures (onionlike nanoparticles, nanotubes) and elegant three-dimensional nanoflowers (NF) have been selectively prepared through an atmospheric pressure chemical vapor deposition (APCVD) process with the reaction of chlorides and sulfur. The morphologies were controlled by adjusting the deposition position, the deposition temperature, and the flux of the carrier gas. All of the nanostructures have been characterized by X-ray powder diffraction (XR… Show more

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...
1

Citation Types

6
102
2

Year Published

2006
2006
2016
2016

Publication Types

Select...
6
1

Relationship

0
7

Authors

Journals

citations
Cited by 153 publications
(110 citation statements)
references
References 71 publications
6
102
2
Order By: Relevance
“…The nanoflowers disassembled into triangular petals (flakes) on sonication with one corner always broken, which suggests that these triangles are connected at only one of the edges to form the assembly of 3D 65 nanoflowers. We observed 10-100's of these triangular petals combining together to form spherical nanoflower structures as suggested by Li et al 22 and evident from the SEM micrograph in reveal mono-and bi-layer regions. This is a significant observation since it highlights that the nanoflowers are composed of few layer nanosheets at the edges.…”
supporting
confidence: 82%
See 3 more Smart Citations
“…The nanoflowers disassembled into triangular petals (flakes) on sonication with one corner always broken, which suggests that these triangles are connected at only one of the edges to form the assembly of 3D 65 nanoflowers. We observed 10-100's of these triangular petals combining together to form spherical nanoflower structures as suggested by Li et al 22 and evident from the SEM micrograph in reveal mono-and bi-layer regions. This is a significant observation since it highlights that the nanoflowers are composed of few layer nanosheets at the edges.…”
supporting
confidence: 82%
“…The nanoflowers disassembled into triangular petals (flakes) on sonication with one corner always broken, which suggests that these triangles are connected at only one of the edges to form the assembly of 3D 65 nanoflowers. We observed 10-100's of these triangular petals combining together to form spherical nanoflower structures as suggested by Li et al 22 and evident from the SEM micrograph in Fig 1a. The nanoflowers are made up of molecular sheets stacked 70 together with a lattice spacing of 3.1 Å and lattice fringes of 0.62 nm, inferred for WS2. In Fig 2a, a cluster of the petals which constitute the nanoflowers is visualised from the edge view (beam perpendicular to c-axis), to reveal 6-8 molecular layers of WS2.…”
supporting
confidence: 82%
See 2 more Smart Citations
“…Apart from the above mentioned synthetic approaches Li et al [47] have developed an atmospheric pressure chemical vapor deposition (APCVD) route for the large …”
Section: Synthesis Of If Nanoparticles and Nanotubes Using Metal Chlomentioning
confidence: 99%