Atomic spectrometry update. Review of advances in the analysis of metals, chemicals and functional materials

Carter, Simon; Fisher, Andrew; García, Raquel; Gibson, Bridget; Lancaster, Steve; Marshall, John; Whiteside, Ian

doi:10.1039/c5ja90045j

Cited by 25 publications

(11 citation statements)

References 262 publications

(216 reference statements)

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“…This latest Update adds to that from last year 1 and complements other reviews 2,3,4,5,6 of analytical techniques in the series of Atomic Spectrometry Updates. Two books which cover elemental speciation have recently been published.…”

Section: Topical Reviewsmentioning

confidence: 79%

Atomic spectrometry update: review of advances in elemental speciation

Clough

Harrington

Hill

et al. 2019

J. Anal. At. Spectrom.

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Section: Topical Reviewsmentioning

confidence: 79%

Atomic spectrometry update: review of advances in elemental speciation

Clough

Harrington

Hill

et al. 2019

J. Anal. At. Spectrom.

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“…Analytical chemistry is one of the most common areas that benefits from the use of chemometric tools. This encompasses a variety of specialized disciplines like materials science, pharmaceuticals, food chemistry, environmental chemistry, biochemistry, and geochemistry . For example, in environmental science, it can used for tracking of impurities and pollutants in water and air.…”

Section: Chemometricsmentioning

confidence: 99%

A Perspective on the Impact of Process Systems Engineering on Reaction Engineering

Sivaramakrishnan

Puliyanda

Tefera

et al. 2019

Ind. Eng. Chem. Res.

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Process systems engineering (PSE), as the name suggests, emphasizes an approach to understanding the behavior of systems as a whole with a view to improving decision-making for optimization and control of processes. The discipline emphasizes the application of mathematical techniques in this effort, and a plausible claim has been made that is at the very core of the discipline of chemical engineering. Being a generalized approach to process systems in general, it finds wide application to many areas in chemical engineering. This work reviews the application of PSE to the area of reaction engineering, which is also at the core of chemical engineering. We highlight the impactful applications of PSE in reaction engineering and discuss aspects of model building and analysis, reactor control, optimization, chemometrics, and chemoinformatics.

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“…Illustration of spectroscopic techniques is fundamental to the undergraduate instrumental analysis course. Atomic spectroscopy is used for elemental analysis in a host of industries including food, energy, environmental, agricultural, and pharmaceutical. − Several instruments are employed including the Atomic Absorption Spectrometer (AAS) and the Inductively Coupled Plasma-Optical Emission Spectrometer (ICP-OES). Laboratory experiments utilizing each have been published in J. Chem.…”

Section: Introductionmentioning

confidence: 99%

“…(AAS, − ICP-OES − ) and collectively demonstrate individual strengths and limitations. A third instrument used for elemental analysis, the Inductively Coupled Plasma–Mass Spectrometer (ICP–MS), has become an academic, industry, and government workhorse for the rapid and nearly simultaneous analysis of most elements in the periodic table at part per trillion (ppt) detection limits or lower. − The experiment described in this work teaches students several important aspects of actual use of this instrument in the laboratory.…”

Section: Introductionmentioning

confidence: 99%

Determination of Arsenic in Sinus Wash and Tap Water by Inductively Coupled Plasma–Mass Spectrometry

et al. 2016

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Arsenic is a toxic element to which humans are primarily exposed through food and water; it occurs as a result of human activities and naturally from the earth's crust. An experiment was developed for a senior level analytical laboratory utilizing an Inductively Coupled Plasma−Mass Spectrometer (ICP−MS) for the analysis of arsenic in household sinus wash and tap water. This powerful instrumental technique can be used to elucidate the elemental composition of a complex sample while offering the benefits of high-precision quantitative analysis. The chosen matrices further provided the opportunity to demonstrate two important analytical concepts. First, the sinus wash samples displayed signal suppression, illustrating the necessity for employment of the internal standard calibration technique. Second, the high chloride matrix of the sinus wash led to the formation of the ArCl + polyatomic ion in the argon plasma, which overlapped with arsenic's single isotope at m/z = 75. Analysis was performed in no gas mode and also with the collision cell in helium mode, allowing the students to observe firsthand the false positive results for arsenic by comparing 75 m/z results in the two modes. In addition, in a third objective, students were able to compare the sinus wash and tap water to current federal drinking water regulations. This laboratory exercise provided a novel and engaging application of ICP−MS and allowed the students to use modern instrumentation and analytical techniques to investigate the current and relevant issue of arsenic in our environment.

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Atomic spectrometry update. Review of advances in the analysis of metals, chemicals and functional materials

Cited by 25 publications

References 262 publications

Atomic spectrometry update: review of advances in elemental speciation

Atomic spectrometry update: review of advances in elemental speciation

A Perspective on the Impact of Process Systems Engineering on Reaction Engineering

Determination of Arsenic in Sinus Wash and Tap Water by Inductively Coupled Plasma–Mass Spectrometry

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