1973
DOI: 10.1007/bf02641359
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Automated determination of silicate and carbonates in detergents

Abstract: The analysis of silicate and carbonate builders in detergents is time consuming by standard gravimetric procedures (1,2). By modifying established Technicon AutoAnalyzer methods, rapid and simple methods of analyzing these detergent builders have been achieved. Standard AutoAnalyzer modules, arranged for colorimetric analysis, are used, and 10–15 samples per hour can be handled. In the silicate analysis, an aqueous solution of the sample is reacted with ammonium molybdate in an acid medium to form silicomolybd… Show more

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Cited by 7 publications
(4 citation statements)
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“…The calculation was carried out following Eq. 3: Greenberg et al (1980), Walinga et al (1989), Navone (1964), ISO 13395 (1996) Nitrite 467 EPA (1974), Greenberg et al (1980), ISO 3696 (1987, ISO 13395 (1996) Ammonia 156 Krom (1980), Searle (1984), ISO 3696 (1987) Phosphate 503 Boltz and Mellon (1948), Greenberg et al (1980), ISO 3696 (1987, Walinga et al (1989), ISO 15681-2 (2003) Silicate 563 Babulak and Gildenberg (1973), Smith andMilne (1981), ISO 3696 (1987), ISO 16264 (2002) Threshold values for both tests were ≥ 0.5 • C for temperature data, ≥ 1 for salinity measurements and ≥ 0.5 mg L −1 for DO content records. Data that passed both tests were, in addition, visually inspected.…”
Section: Temperature Salinity and Dissolved Oxygenmentioning
confidence: 99%
“…The calculation was carried out following Eq. 3: Greenberg et al (1980), Walinga et al (1989), Navone (1964), ISO 13395 (1996) Nitrite 467 EPA (1974), Greenberg et al (1980), ISO 3696 (1987, ISO 13395 (1996) Ammonia 156 Krom (1980), Searle (1984), ISO 3696 (1987) Phosphate 503 Boltz and Mellon (1948), Greenberg et al (1980), ISO 3696 (1987, Walinga et al (1989), ISO 15681-2 (2003) Silicate 563 Babulak and Gildenberg (1973), Smith andMilne (1981), ISO 3696 (1987), ISO 16264 (2002) Threshold values for both tests were ≥ 0.5 • C for temperature data, ≥ 1 for salinity measurements and ≥ 0.5 mg L −1 for DO content records. Data that passed both tests were, in addition, visually inspected.…”
Section: Temperature Salinity and Dissolved Oxygenmentioning
confidence: 99%
“…Total oxidized nitrogen concentrations (NO x ) were determined by the cadmium reduction method, followed by measurement of nitrite (originally present plus reduced nitrite). Greenberg et al, 1980;Walinga et al, 1989;Navone, 1964;ISO 13395, 1996Nitrite 467 EPA, 1974Greenberg et al, 1980;ISO 3696, 1987;ISO 13395, 1996Ammonia 156 Krom, 1980Searle, 1984;ISO 3696, 1987 Phosphate 503 Boltz andMellon, 1948;Greenberg et al, 1980;ISO 3696, 1987;Walinga et al, 1989;ISO 15681-2, 2003 Silicate 563 Babulak and Gildenberg, 1973;Smith and Milne, 1981;ISO 3696, 1987;ISO 16264, 2002…”
Section: Nutrient Sampling and Analysismentioning
confidence: 99%
“…The calculation was carried out following Eq. (3): (1974), Greenberg et al (1980), ISO 3696 (1987, ISO 13395 (1996) Ammonia 156 Krom (1980), Searle (1984), ISO 3696 (1987) Phosphate 503 Boltz and Mellon (1948), Greenberg et al (1980), ISO 3696 (1987), Walinga et al (1989), ISO 15681-2 (2003) Silicate 563 Babulak and Gildenberg (1973), Smith and Milne (1981), ISO 3696 (1987), ISO 16264 (2002) Threshold values for both tests were ≥ 0.5 • C for temperature data, ≥ 1 for salinity measurements and ≥ 0.5 mg L −1 for DO content records. Data that passed both tests were, in addition, visually inspected.…”
Section: Temperature Salinity and Dissolved Oxygenmentioning
confidence: 99%