2014
DOI: 10.1002/jssc.201400634
|View full text |Cite
|
Sign up to set email alerts
|

Automated headspace solid-phase microextraction and on-fiber derivatization for the determination of clenbuterol in meat products by gas chromatography coupled to mass spectrometry

Abstract: A method was developed for the determination of clenbuterol in meat using stable-isotope-dilution gas chromatography with mass spectrometry coupled with solid-phase microextraction and on-fiber derivatization. The samples were first homogenized with hydrochloric acid followed by protein deposition. After headspace solid-phase microextraction and on-fiber derivatization, the content of clenbuterol was measured with the aid of stable-isotope dilution. The condition of solid-phase microextraction was optimized by… Show more

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...
5

Citation Types

0
12
0

Year Published

2015
2015
2017
2017

Publication Types

Select...
6

Relationship

1
5

Authors

Journals

citations
Cited by 20 publications
(12 citation statements)
references
References 38 publications
0
12
0
Order By: Relevance
“…Gas chromatography–mass spectrometry (GC‐MS) coupled with solid‐phase microextraction (SPME) has been successfully employed for the qualitative and quantative analysis of volatile and semivolatile compounds in many fields, such as the determination of fruits (Jiang, Ni, Zhu, & Zhu, ; Nardini et al, ; Perestrelo, Barros, Rocha, & Câmara, ), fruit juice (Balme & Gülaçar, ), vegetables (Murat, Gourrat, Jerosch, & Cayot, ), meat (Jiang & Ni, ), wines (Burin, Marchand, De Revel, & Bordignon‐Luiz, ), and plants (Chai et al, ). SPME was introduced first by Arthur and Pawlizyn (Arthur & Pawliszyn, ) in 1990, which integrates sampling, extraction, concentration, and sample introduction to GC.…”
Section: Introductionmentioning
confidence: 99%
“…Gas chromatography–mass spectrometry (GC‐MS) coupled with solid‐phase microextraction (SPME) has been successfully employed for the qualitative and quantative analysis of volatile and semivolatile compounds in many fields, such as the determination of fruits (Jiang, Ni, Zhu, & Zhu, ; Nardini et al, ; Perestrelo, Barros, Rocha, & Câmara, ), fruit juice (Balme & Gülaçar, ), vegetables (Murat, Gourrat, Jerosch, & Cayot, ), meat (Jiang & Ni, ), wines (Burin, Marchand, De Revel, & Bordignon‐Luiz, ), and plants (Chai et al, ). SPME was introduced first by Arthur and Pawlizyn (Arthur & Pawliszyn, ) in 1990, which integrates sampling, extraction, concentration, and sample introduction to GC.…”
Section: Introductionmentioning
confidence: 99%
“…As a simple, sensitive, and solvent-free technique, HS-SPME has been widely applied to determine the volatile compositions of medicines [34,35], drink [36][37][38], food [39,40], and fruits [41][42][43].…”
Section: Introductionmentioning
confidence: 99%
“…Headspace solid‐phase microextraction (HS‐SPME) is a sampling and concentration technique for analysis of volatile and semi‐volatile substances in a large variety of matrices. As a simple, sensitive, and solvent‐free technique, HS‐SPME has been widely applied to determine the volatile compositions of medicines , drink , food , and fruits .…”
Section: Introductionmentioning
confidence: 99%
“…β 2 ‐Agonists, such as salbutamol (SAL) and clenbuterol (CLE), are a class of veterinary drugs used in food‐producing animals to promote leanness of meat . The illegal abuse of β 2 ‐agonists in breeding is detrimental to both animal and human health by inducing heart palpitations, diarrhea, muscle tremors, and even malignant tumors .…”
Section: Introductionmentioning
confidence: 99%