1991
DOI: 10.1007/bf02657683
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Bisoxathiolane sulfides from a dioxoene fatty acid

Abstract: A quantitative preparation of bisoxathiolane from 9,12-dioxo-trans-10-octadecenoic acid is discussed. The reagents used are fl-mercaptoethanol and BF 3etherate in acetic acid. The structure of the product was established with the help of elemental analysis, infrared, nuclear magnetic resonance and mass spectroscopy data.

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Cited by 5 publications
(3 citation statements)
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“…The 1,3-dipolar cycloaddition reaction with nitrile oxides (10-13) is a facile method for the preparation of isoxazolines (14,15). The present work is a continuation of our studies on introducing novel heterocyclic moieties into fatty acid chains (16)(17)(18)(19). Here, we report the reaction of methyl 10-undecenoate (I) and methylcis-9-octadecenoate (II) with methoxy carbonyl formonitrile oxide.…”
mentioning
confidence: 93%
“…The 1,3-dipolar cycloaddition reaction with nitrile oxides (10-13) is a facile method for the preparation of isoxazolines (14,15). The present work is a continuation of our studies on introducing novel heterocyclic moieties into fatty acid chains (16)(17)(18)(19). Here, we report the reaction of methyl 10-undecenoate (I) and methylcis-9-octadecenoate (II) with methoxy carbonyl formonitrile oxide.…”
mentioning
confidence: 93%
“…The oxathiolanes and their derivatives are useful as pesticides {4) and in neoplastic therapy (5). Earlier, we reported the preparation of fatty acid analogues containing such heterocycles (7)(8)(9)(10). Earlier, we reported the preparation of fatty acid analogues containing such heterocycles (7)(8)(9)(10).…”
mentioning
confidence: 99%
“…Spirooxathiolane derivatives are diagnostic agents in the central nervous or cholinergic system (6). Earlier, we reported the preparation of fatty acid analogues containing such heterocycles (7)(8)(9)(10). Scanning the literature revealed to us that thiazole or oxathiolane rings fused with other heterc~ cyclic systems are not well known in fatty acid chemistry.…”
mentioning
confidence: 99%